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【新文速递】2025年2月24日复合材料SCI期刊最新文章

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今日更新:Composite Structures 5 篇,Composites Part A: Applied Science and Manufacturing 2 篇,Composites Part B: Engineering 1 篇,Composites Science and Technology 2 篇

Composite Structures

Influence of geometry on in-plane and out-of-plane wave propagation of 2D hexagonal and re-entrant lattices

Somraj Sen, Arindam Das, Indrajit Pahari, Arnab Banerjee

doi:10.1016/j.compstruct.2025.118958

几何形状对二维六边形和可重入格面内和面外波传播的影响

The evaluation of the dispersion characteristics, including iso-frequency contours, group velocity maps, and directivity plots, are presented for 2D periodic lattices with varying internal angles. This study delves into the wave propagation behavior of various lattices to understand the emergence of wave directionality through variations in geometry, particularly internal angles, considering both in-plane and out-of-plane deformations. The spectral element formulation is used to model each lattice member considering space frame elements. The Bloch-Floquet theorem is employed to establish the dispersion relationships after defining the periodicity of unit cells. Detailed analysis manifests that isofrequency contours become more concave as internal angles decrease, indicating high directionality in re-entrant lattices. This is confirmed by directivity plots and group velocity maps. Modes, namely axial, flexural, and torsional modes are identified for the regular hexagonal lattice. Further, Dirac cones are observed for the hexagonal lattice. Notably, a directional roton-like phenomenon is discovered, displaying both negative and positive group velocities for specific wave packets. These findings have potential applications for wave manipulation and control, particularly in acoustics and vibration control.

本文给出了具有不同内角的二维周期晶格的色散特性的评价,包括等频等高线、群速度图和指向性图。本研究深入研究了各种晶格的波传播行为,以了解通过几何变化,特别是内角,考虑到面内和面外变形,波的方向性的出现。考虑空间框架元素,采用谱元公式对每个格元进行建模。在定义了单元格的周期性后,利用Bloch-Floquet定理建立了色散关系。详细分析表明,随着内角的减小,等频轮廓变得更加凹,表明在重入格中具有较高的方向性。指向性图和群速度图证实了这一点。正六边形晶格的模态,即轴向、弯曲和扭转模态。此外,在六边形晶格中观察到狄拉克锥。值得注意的是,发现了一种方向性的类似旋转的现象,显示了特定波包的负和正群速度。这些发现在波浪操纵和控制方面具有潜在的应用,特别是在声学和振动控制方面。


Modeling of variable angle tow composites using a variable separation method based on a unified formulation

P. Vidal, G. Giunta, D.A. Iannotta, L. Gallimard, O. Polit

doi:10.1016/j.compstruct.2025.118963

基于统一公式的可变分离变角度复合材料建模

In this article, we are interested in the modeling of variable stiffness plate structures through a variable separation approach. The displacement field is approximated as a sum of separated functions of the in-plane coordinates x, y and the transverse coordinate z. A non-linear problem is derived. It can be solved using an iterative process involving 2D and 1D linear problems successively. To keep the separability feature ensuring a computational efficiency, the so-called Carrera’s Unified Formulation (CUF) is adapted to our framework. Classical Finite Element method is used. In the thickness direction, a fourth-order expansion in each layer is considered. The number of unknowns is reduced compared to classical LayerWise (LW) approach. Test cases encountered in the literature are provided to assess the present LW method and compare the results with reference solutions. Laminated and sandwich structures with different slenderness ratios and variations of angle tows are addressed. Very satisfacfory results with a low computational cost are obtained.

在本文中,我们通过变量分离法对变刚度板结构进行建模。位移场被近似为平面内坐标 x、y 和横向坐标 z 的分离函数之和。由此推导出一个非线性问题,该问题可通过依次求解二维和一维线性问题的迭代过程来解决。为了保持可分离性特征以确保计算效率,我们对所谓的卡雷拉统一公式(CUF)进行了调整以适应我们的框架。采用经典的有限元法。在厚度方向上,每层考虑四阶展开。与经典的层合(LW)方法相比,未知数的数量减少了。提供了文献中遇到的测试案例,以评估当前的 LW 方法,并将结果与参考解进行比较。研究了具有不同长细比和角度层变化的层合和夹层结构。获得了计算成本低且非常令人满意的成果。


Inverse design of lattice metamaterials for fully anisotropic elastic constants: A data-driven and gradient-based method

Zixing Fu, Huina Mao, Binglun Yin

doi:10.1016/j.compstruct.2025.118975

完全各向异性弹性常数的晶格超材料的反设计:数据驱动和基于梯度的方法

The elastic constant tensor and its anisotropy are among the most critical mechanical properties, as they govern numerous mechanical phenomena and are prevalent in many natural materials. However, the efficient and accurate inverse design of metamaterials with desired elastic constants remains challenging, particularly for fully anisotropic elastic constants with low symmetries. Recent advances in artificial intelligence have opened new avenues to address this challenge. In this work, we propose a general framework that combines data-driven artificial neural networks with a gradient-based optimization algorithm to achieve high-precision inverse design of fully anisotropic elastic constants, exemplified using open cellular lattice Kelvin cells. First, an automatic parametric finite element method is introduced to calculate the elastic constants of any (distorted) Kelvin cells. Next, neural networks are developed to approximate the computationally costly finite element method, acting as the forward characterization function in the design process. Finally, an inverse design framework that integrates neural networks with a gradient-based optimization algorithm is proposed and validated. The successful design outcomes in practical examples, such as artificial bone implants and structures with unconventional Poisson’s ratios, demonstrate the capability of our method to guide high-precision inverse design across various engineering applications.

弹性常数张量及其各向异性是最关键的力学性能之一,因为它们控制着许多力学现象,并普遍存在于许多天然材料中。然而,具有理想弹性常数的超材料的有效和精确的反设计仍然具有挑战性,特别是对于具有低对称性的完全各向异性弹性常数。人工智能的最新进展为解决这一挑战开辟了新的途径。在这项工作中,我们提出了一个通用框架,将数据驱动的人工神经网络与基于梯度的优化算法相结合,以实现完全各向异性弹性常数的高精度反设计,例如使用开放细胞晶格开尔文细胞。首先,引入一种自动参数有限元方法来计算任意(畸变)开尔文单元的弹性常数。其次,开发神经网络来近似计算成本高昂的有限元方法,作为设计过程中的前向表征函数。最后,提出并验证了将神经网络与梯度优化算法相结合的逆向设计框架。在实际例子中,如人工骨植入物和非常规泊松比结构的成功设计结果,证明了我们的方法在各种工程应用中指导高精度逆设计的能力。


Experimental compressive damage analysis on holed laminates under dynamic loadings using in-situ MHz synchrotron X-ray phase contrast imaging

J.M. Rodríguez-Sereno, J. Pernas-Sánchez, J.A. Artero-Guerrero, A. Rack, A. Vaz-Romero, J. López-Puente, D. Varas, F. Naya, A. Cohen, B. Lukić

doi:10.1016/j.compstruct.2025.118978

利用原位MHz同步x射线相衬成像技术分析动载荷作用下多孔层压板的压缩损伤

This study highlights the importance of investigating the behavior of the inner layers of carbon fiber-reinforced polymer (CFRP) laminates under dynamic compression, using Synchrotron-based techniques to understand damage initiation and failure propagation at high strain rates. Open and filled hole specimens with three different CFRP architectures were tested using the Split Hopkinson Pressure Bar (SHPB). Digital image correlation (DIC) and Synchrotron-based X-ray MHz radiography were performed simultaneously with ultra high-speed cameras (two Shimadzu HPV-X2 for X-ray images and one Photron SAZ for visible light). This allowed the first observation of matching outer and inner failures with surface strain fields at a micrometer level. Results showed that, in certain conditions, failure initiated earlier in the inner layers, leading to through-thickness propagation. This correlation between strength and internal damage initiation might be overlooked if only outer visible light images are used. The proposed methodology, which emphasized post-processing of X-ray images, can serve as a baseline for future research on the behavior of inner layers of composite materials under high strain rates. Additionally, analysis of different CFRP architectures revealed their influence on unloading time after initial failure.

这项研究强调了研究碳纤维增强聚合物(CFRP)层压板内层在动态压缩下的行为的重要性,使用基于同步加速器的技术来了解高应变率下的损伤起裂和失效扩展。采用分离式霍普金森压杆(SHPB)对三种不同CFRP结构的开孔和填孔试件进行了测试。采用超高速相机(两台Shimadzu HPV-X2拍摄x射线图像,一台Photron SAZ拍摄可见光图像)同时进行数字图像相关(DIC)和基于同步加速器的x射线MHz摄影。这使得首次观察到在微米水平上匹配表面应变场的外部和内部失效。结果表明,在一定条件下,内层的破坏开始得更早,导致了穿层扩展。如果只使用外部可见光图像,强度和内部损伤之间的相关性可能会被忽略。所提出的方法强调了x射线图像的后处理,可以作为未来研究复合材料内层在高应变率下行为的基线。此外,分析了不同CFRP结构对初始破坏后卸载时间的影响。


Composites Part A: Applied Science and Manufacturing

Impact damage detection on carbon fiber reinforced polymer tube by a mutual differential Bobbin probe

Wei Guo, Lihua Guo, Hao Xu, Weijun Zhu, Shejuan Xie, Zhenmao Chen, Toshiyuki Takagi, Tetsuya Uchimoto

doi:10.1016/j.compositesa.2025.108806

用互差筒管探头检测碳纤维增强聚合物管的冲击损伤

Carbon fiber reinforced polymer (CFRP) tube is utilized in large aperture deployable space antennas for its superior material properties. Impact damages on CFRP tube can significantly impair the load-bearing capacity of the tubes. Efficient and convenient non-destructive evaluation method of impact damage in CFRP tubes is essential. This study develops a high-frequency eddy current testing (HF ECT) finite element analysis method that accounts for both the dielectric properties and anisotropic conductivity of CFRP, and establishes a fiber bundle model that explains the operating mechanism of displacement current and eddy currents in CFRP, offering guidance for predicting HF ECT signals in CFRP. A high signal-to-noise ratio mutual differential Bobbin probe is developed specifically for detecting impact damage in CFRP tubes. A HF ECT experiment system is constructed and validated using impact damages induced by a force hammer, demonstrating the effectiveness of method and probe, and the invisible impact defect is detected successfully.

碳纤维增强聚合物(CFRP)管以其优越的材料性能被应用于大孔径可展开空间天线中。CFRP钢管的冲击损伤会严重影响钢管的承载能力。高效、便捷的CFRP管材冲击损伤无损评价方法是至关重要的。本研究发展了同时考虑CFRP介电性能和各向异性电导率的高频涡流测试(HF ECT)有限元分析方法,并建立了解释CFRP中位移电流和涡流作用机理的纤维束模型,为预测CFRP中高频ECT信号提供指导。研制了一种高信噪比互差筒管探头,专门用于检测CFRP管的冲击损伤。利用力锤冲击损伤构建了高频电刺 激实验系统并进行了验证,验证了方法和探头的有效性,成功检测出了不可见的冲击缺陷。


Co-training of multiple neural networks for simultaneous optimization and training of physics-informed neural networks for composite curing

Keith D. Humfeld, Geun Young Kim, Ji Ho Jeon, John Hoffman, Allison Brown, Jonathan Colton, Shreyes Melkote, Vinh Nguyen

doi:10.1016/j.compositesa.2025.108820

 

复合材料固化过程中多个神经网络同时优化的协同训练和物理信息神经网络的训练

This paper introduces a Physics-Informed Neural Network (PINN) technique that co-trains neural networks (NNs) that represent each function in a system of equations to simultaneously solve equations representing an out-of-autoclave (OOA) cure process while conducting optimization in adherence to process requirements. Specifically, this co-training approach benefits from using NNs to represent OOA inputs (air temperature profile) and outputs (part and tool temperature profiles and degree of cure). Production requirements can then be levied on the inputs, such as maximum air temperature and minimum cure cycle, and simultaneously on the outputs, such as degree of cure, maximum part temperature, and part temperature rate limits. Co-training the NNs results in an optimized input producing outputs that meet all OOA process requirements. The technique is validated with finite element (FE) simulations and physical experiments for curing a Toray T830H-6 K/3900-2D composite panel. Hence, this novel approach efficiently models and optimizes the OOA cure process.

本文介绍了一种物理信息神经网络(PINN)技术,该技术共同训练代表方程系统中每个函数的神经网络(nn),以同时求解代表高压灭菌器外(OOA)固化过程的方程,同时根据工艺要求进行优化。具体来说,这种协同训练方法得益于使用神经网络来表示OOA输入(空气温度曲线)和输出(零件和工具温度曲线以及固化程度)。然后,可以对输入进行生产要求,例如最高空气温度和最低固化周期,同时对输出进行生产要求,例如固化程度、最高部件温度和部件温度速率限制。共同训练神经网络的结果是一个优化的输入,产生满足所有OOA过程要求的输出。通过对东丽T830H-6 K/3900-2D复合材料板的有限元模拟和物理实验验证了该技术的有效性。因此,这种新方法有效地建模和优化了OOA固化过程。


Composites Part B: Engineering

Shear behavior and strain transmission mechanism in bonding interface of robust toughened epoxy/flattened bamboo composites

Qingdi Jia, Mingjie Guan, Shuai Qian, Mengyu Wu, Pulin Che, Xu Liu

doi:10.1016/j.compositesb.2025.112334

 

坚固增韧环氧树脂/扁平竹复合材料界面剪切行为及应变传递机理

To improve the brittle bonding interface of epoxy/flattened bamboo composite (EFB) and expand its application in bamboo buildings, the effects of bonding structures, alkali-treated surface, and toughened epoxy on shear bonding behavior of EFB were systemically investigated to completely understand bonding interface mechanism and novelly simulated models was analyzed. The microstructure and chemical bonding group of the EFB bonding interface were characterized to reveal the toughening bonding mechanisms. The tensile shear behavior of the bonding interface was analyzed by digital image correlation (DIC) and the strain transfer mechanism was simulated by finite element analysis (FEA). Results indicated that the bonding interphase between epoxy and flattened bamboo primarily involved mechanical interlocking in the bonding interface and chemical bonding in the parenchyma cells. The alkali-treated surface and toughened epoxy group (ATEG) improved epoxy penetration on flattened bamboo surface changing the interphase between epoxy and bamboo interface. Alkali-treated surface and toughened epoxy significantly enhanced shear strength and fracture energy of EFB. The maximum dry shear strength of ATEG was higher than control group, with increases varying across the three bonding structures. Under hygrothermal conditions, ATEG achieved the highest wet shear strength in core-reinforced structure with bamboo failure of 60%. DIC analysis revealed the improvement of strain continuity and dispersion in ATEG under dry conditions, while strain concentration occurred mainly in interphase of EFB bonding interface under hygrothermal conditions leading to the debonding failure. FEA illustrated that alkali-treated surface and toughened epoxy reduced strain concentration in the interphase of bonding interface and improved strain distribution of EFB, consistent with DIC analysis.

为改善环氧/扁平竹复合材料的脆性粘结界面,扩大其在竹建筑中的应用,系统研究了粘结结构、碱处理表面和增韧环氧树脂对环氧/扁平竹复合材料剪切粘结行为的影响,以全面了解环氧/扁平竹复合材料的粘结界面机理,并建立了新的模拟模型。通过对EFB结合界面的微观结构和化学结合基团的表征,揭示了其增韧结合机理。采用数字图像相关(DIC)分析了粘结界面的拉伸剪切行为,并采用有限元分析(FEA)模拟了应变传递机理。结果表明,环氧树脂与扁平竹的键合界面主要为键合界面的机械互锁和薄壁细胞的化学键合。碱处理表面和增韧环氧基(ATEG)改善了环氧树脂在扁平竹表面的渗透,改变了环氧树脂与竹界面的界面相。碱处理表面和增韧环氧树脂显著提高了EFB的抗剪强度和断裂能。ATEG的最大干抗剪强度高于对照组,三种粘结结构的最大干抗剪强度均有所增加。在湿热条件下,ATEG在竹破坏率为60%的核心钢筋结构中湿抗剪强度最高。DIC分析显示,干燥条件下ATEG的应变连续性和分散性得到改善,而湿热条件下应变集中主要发生在EFB粘结界面界面,导致脱粘失效。有限元分析结果表明,碱处理表面和增韧环氧树脂降低了键合界面界面的应变浓度,改善了EFB的应变分布,与DIC分析结果一致。


Composites Science and Technology

Comparative Analysis of NOL-Ring Tensile Strength in Towpreg and Slit-Tape for Filament Winding: Influence of Resin Viscosity, Tack, and Consolidation

Eduardo Szpoganicz, Fabian Hübner, Marius Luik, Jeremias Thomas, Florian Max, Andreas Scherer, Tobias Dickhut, Holger Ruckdäschel

doi:10.1016/j.compscitech.2025.111123

 

长丝卷绕用丝带和开缝带no - ring抗拉强度的对比分析:树脂粘度、粘性和固结的影响

This study investigates the tensile strength of carbon-fiber reinforced polymer (CFRP) specimens manufactured via filament winding with varying winding parameters. NOL-rings (Naval Ordnance Laboratories) were processed using unidirectional CFRP material, and the performance of towpregs was compared to slit-tapes of different widths and temperature settings. To establish a benchmark, autoclave-cured prepregs were laminated into flat rectangular samples. The manufacturing process revealed significant variations in laminate strength and ply consolidation, analyzed through optical micrographs and profile analysis. Tensile strengths of the NOL-rings ranged from 1430 MPa to 1800 MPa, with towpregs performing better due to higher tackiness and improved consolidation, compared to slit-tapes with no applied temperature. However, both were still bellow the 2100 MPa strength of autoclave-cured reference samples. Finite element analysis showed that the NOL-ring geometry induces bending stresses, even in an idealized part, reducing the theoretical tensile strength to 1900 MPa. Additionally, in-situ cryogenic testing using liquid nitrogen was reported for the first time for NOL-ring specimens, revealed a significant increase in strength to 2200 MPa, attributed to the stiffening effect at low temperatures. This work introduces a novel approach by correlating ply consolidation with slit-tapes, towpregs, and winding parameters, linking prepreg tackiness to tensile performance, and presenting additionally testing of NOL-rings at 77 K, thus providing understanding of their behavior in cryogenic environments.

研究了不同缠绕参数下碳纤维增强聚合物(CFRP)长丝缠绕试样的拉伸强度。采用单向CFRP材料加工no -rings (Naval ororance Laboratories),并将其与不同宽度和温度设置的缝带的性能进行了比较。为了建立一个基准,蒸压固化的预浸料被层压成扁平的矩形样品。通过光学显微照片和剖面分析,制造过程揭示了层压强度和层压固结的显著变化。nol环的抗拉强度从1430 MPa到1800 MPa不等,与没有施加温度的缝带相比,拖带具有更高的粘性和更好的固结性,因此性能更好。然而,两者的强度仍低于蒸压罐固化参考样品的2100 MPa。有限元分析表明,即使在理想的零件上,NOL-ring几何形状也会产生弯曲应力,使理论抗拉强度降低到1900 MPa。此外,首次报道了使用液氮对no -ring试件进行的原位低温测试,结果显示,由于低温下的硬化效应,no -ring试件的强度显著提高至2200 MPa。这项工作介绍了一种新的方法,通过将胶层固结与缝带,带浸料和缠绕参数相关联,将预浸料粘性与拉伸性能联系起来,并在77 K下进行了noll环的额外测试,从而了解了它们在低温环境中的行为。


Macro/Micro Synergistic Thermal Conductivity Enhancement in Liquid Metal-Based Phase Change Composites for Thermal Management in Electronic Devices

Guangyin Liu, Kaixun Shang, Shiqi Chen, Jun Shen

doi:10.1016/j.compscitech.2025.111120

 

用于电子器件热管理的液态金属基相变复合材料的宏/微协同导热增强

Liquid metals (LM) demonstrate significant potential in thermal management applications for electronic devices due to their high thermal conductivity and phase change heat absorption capabilities. However, when combined with organic flexible substrates to create composite materials, the advantages of high thermal conductivity can be substantially diminished. To address this challenge, this study proposes a macro/micro synergistic thermal conductivity enhancement method. By coating LM particles with carbon nanotubes (CNT), the LM@CNT particles that mimics a "neuron" structure was developed. LM@CNT was combined with silicone rubber (SR) to form the LM@CNT/SR, which exhibits micro-level thermal conductivity enhancement. The integration of LM@CNT in SR establishes a thermal conduction network, resulting in a thermal conductivity of 1.37 W/m/K for the LM@CNT/SR. Inspired by the growth rings in tree trunks, vertically aligned graphene films (VAGF) are ingeniously embedded in the composite material to enhance thermal conductivity at the macro-level. The results show that embedding 0.02 mm thick VAGF can increase thermal conductivity by 8.8 W/m/K, while 0.1 mm thick VAGF can achieve an increase of 24.7 W/m/K. The thermal conductivity of LM@CNT/SR/VAGF has obvious anisotropy. Furthermore, the LM@CNT/SR/VAGF demonstrates excellent stability, with negligible changes in thermal conductivity after nearly 2000 temperature cycles. The methodology proposed in this study for producing high thermal conductivity phase change composite materials employs simple and cost-effective processes, offering a novel framework for the mass production of such composites. This approach shows substantial potential for applications in thermal surge protection and thermal management within electronic devices.

液态金属(LM)由于其高导热性和相变吸热能力,在电子器件的热管理应用中显示出巨大的潜力。然而,当与有机柔性基板结合以创建复合材料时,高导热性的优点可以大大减少。为了解决这一挑战,本研究提出了一种宏观/微观协同增强导热系数的方法。通过用碳纳米管(CNT)涂覆LM颗粒,开发了模拟“神经元”结构的LM@CNT颗粒。LM@CNT与硅橡胶(SR)结合形成LM@CNT/SR,具有微级导热性能增强。LM@CNT在SR中的集成建立了一个导热网络,使得LM@CNT/SR的导热系数为1.37 W/m/K。受树干年轮的启发,垂直排列的石墨烯薄膜(VAGF)巧妙地嵌入复合材料中,以增强宏观上的导热性。结果表明,嵌入0.02 mm厚的VAGF可使导热系数提高8.8 W/m/K,而0.1 mm厚的VAGF可使导热系数提高24.7 W/m/K。LM@CNT/SR/VAGF的导热系数具有明显的各向异性。此外,LM@CNT/SR/VAGF表现出优异的稳定性,在近2000次温度循环后,导热系数的变化可以忽略不计。本研究中提出的生产高导热相变复合材料的方法采用简单且具有成本效益的工艺,为大规模生产此类复合材料提供了新的框架。这种方法在电子设备的热涌保护和热管理方面显示出巨大的应用潜力。




来源:复合材料力学仿真Composites FEM
ACTMechanicalOpticalSystemInspire振动断裂复合材料非线性化学光学通用建筑电子理论材料人工智能
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【新文速递】2025年2月23日复合材料SCI期刊最新文章

今日更新:Composite Structures 4 篇,Composites Part A: Applied Science and Manufacturing 1 篇,Composites Part B: Engineering 5 篇Composite StructuresFree vibrations and buckling analyses of sandwich cylindrical shells with auxetic core and shape memory alloy wires reinforced face sheetsFarzan Yavari, Akbar Alibeigloodoi:10.1016/j.compstruct.2025.118994形状记忆合金线增强面板带辅助芯夹层圆柱壳的自由振动和屈曲分析In this study, free vibrations and buckling analyses of cylindrical sandwich shells with an auxetic honeycomb core and shape memory alloy (SMA) wires reinforced face sheets in thermal environments were conducted. The properties of the shape memory alloy wires were calculated using the one-dimensional Brinson model. The equations of motion were derived based on classical theory, considering Von-Karman geometric nonlinearity and utilizing Hamilton’s principle. The linearized and homogenized equations of motion, obtained through the perturbation technique, were solved using the differential quadrature method to determine the structure’s natural frequency and buckling load. The results were validated by comparing them with existing literature. The effects of the geometrical parameters of the structure, the volume fraction and pre-strain of the wires, and temperature on the natural frequency, buckling load, and thermal buckling were investigated. The results showed that by embedding honeycomb cells or wires in the circumferential direction of the cylinder, high natural frequencies can be achieved, while embedding them in the longitudinal direction creates high buckling load and thermal buckling. Additionally, increasing the pre-strain and volume fraction of the wires enhances the natural frequency, buckling load, and thermal buckling.在本研究中,对具有消声蜂窝芯的圆柱形夹层壳和形状记忆合金(SMA)丝增强面板在热环境下的自由振动和屈曲进行了分析。采用一维Brinson模型对形状记忆合金丝的性能进行了计算。在经典理论的基础上,考虑Von-Karman几何非线性,利用Hamilton原理推导出了运动方程。通过摄动技术得到线性化和均匀化的运动方程,采用微分正交法求解,确定了结构的固有频率和屈曲载荷。通过与已有文献的比较,验证了研究结果。研究了结构几何参数、丝的体积分数、预应变、温度对固有频率、屈曲载荷和热屈曲的影响。结果表明,在圆柱体周向埋设蜂窝单元或蜂窝丝可以获得较高的固有频率,而在纵向埋设蜂窝单元或蜂窝丝会产生较高的屈曲载荷和热屈曲。此外,增加钢丝的预应变和体积分数可以提高固有频率、屈曲载荷和热屈曲。Effect of prepreg ply thickness and orientation on tensile properties and damage onset in carbon-fiber composites for cryogenic environmentsEduardo Szpoganicz, Fabian Hübner, Uwe Beier, Matthias Geistbeck, Maximilian Korff, Ling Chen, Youhong Tang, Tobias Dickhut, Holger Ruckdäscheldoi:10.1016/j.compstruct.2025.118996 预浸料厚度和取向对低温环境下碳纤维复合材料拉伸性能和损伤发生的影响This study addresses the effects of laminate design on the damage and failure behaviour of carbon-fiber reinforced composites with varying ply thicknesses and stacking configurations under cryogenic temperatures. The aim was to observe the ultimate tensile performance and in-situ onset of damage at 296 and 77 K environments, combining microscopy and simulation analyses. Laminates with fiber areal weights of 140, 70 and 45 g/m2 were stacked in 2 different quasi-isotropic configurations. The results show that ultimate tensile properties are improved at 77 K, though failure strain slightly decreases. Thinner ply laminates with 70 and 45 g/m2 showed a 15–20 % improvement in cryogenic tensile failure-strain, while damage onset shifted from 0.5 % to 0.8 % of strain. Adding off-axis plies improved laminates by 10–15 %, preventing damage onset up to failure. Microscopy and simulation analyses showed good agreement with the in-situ signal for the onset of damage, indicating matching levels of delamination failure initiation measured at 77 K. No transverse microcracks were observed, and permeation measurements showed no significant leakage increase after delamination onset. Ultimately, this work introduces a novel integrated approach by combining in-situ cryogenic testing, damage onset methodology, fractography, simulation analysis, and gas permeation measurements.本研究探讨了层压设计对不同厚度碳纤维增强复合材料在低温下的损伤和破坏行为的影响。目的是结合显微镜和模拟分析,观察296和77 K环境下的极限拉伸性能和原位损伤。纤维面重分别为140、70和45 g/m2的层压板以2种不同的准各向同性构型堆叠。结果表明:77 K的极限拉伸性能得到改善,但破坏应变略有降低;厚度为70和45 g/m2的较薄层合板在低温拉伸破坏应变方面表现出15-20 %的改善,而损伤开始从应变的0.5 %转变为0.8 %。添加离轴层改善了10-15 %的层压板,防止损坏发生直到失败。显微镜和模拟分析显示,损伤开始的原位信号与77 K测量的分层破坏起始水平相匹配。没有观察到横向微裂纹,渗透率测量显示分层发生后泄漏量没有明显增加。最后,这项工作引入了一种新的综合方法,将原位低温测试、损伤发生方法、断口学、模拟分析和气体渗透测量相结合。Experimental study of bond performance on carbon fiber fabric-steel joint with mechanical anchors at elevated temperaturesZhongwei Zhao, Zeyuan Jindoi:10.1016/j.compstruct.2025.118998高温机械锚固碳纤维-钢连接粘结性能试验研究This paper investigates the effects of anchor reinforcement on the bond-slip behavior of carbon fiber fabric-steel systems under high-temperature conditions. The experiments were conducted with three temperature ranges from 20 °C to 70 °C, including a control group with no anchor reinforcement and two groups with different anchor positions. The results indicated that as the temperature increased from 20 °C to 50 °C, the load capacity of all specimen groups improved to varying extents. Beyond 50 °C, a significant degradation in load capacity was observed for all groups. Furthermore, temperature and anchor position significantly affected the failure modes, including the residual area of carbon fiber fabric on the steel plate surface (RA) and the modes of carbon fiber fabric fracture, as well as the bond-slip behavior. As the temperature rose, but the glass transition temperature (Tg ), RA increased, impacting the strain distribution and the maximum shear stress at the bonded interface. The experiments also showed that when the environmental temperature exceeds Tg , anchor reinforcement can enhance the bond reliability of the carbon fiber fabric-steel system. The findings of this study provide insights into the degradation patterns of carbon fiber fabric-steel under high-temperature environments and propose a viable reinforcement method.本文研究了高温条件下锚固加固对碳纤维-钢体系粘结滑移性能的影响。实验在20 °C ~ 70 °C的三个温度范围内进行,包括没有锚固加固的对照组和不同锚固位置的两组。结果表明:当温度从20 °C升高到50 °C时,各组试件的承载能力均有不同程度的提高。超过50 °C,所有组的负载能力都明显下降。温度和锚固位置显著影响碳纤维织物在钢板表面的残余面积(RA)和碳纤维织物的断裂模式,以及粘结滑移行为。随着温度的升高,玻璃化转变温度(Tg ), RA增大,影响了粘结界面处的应变分布和最大剪切应力。实验还表明,当环境温度超过Tg时 锚固加固可以提高碳纤维-钢结构的粘结可靠性。研究结果揭示了碳纤维-钢复合材料在高温环境下的降解规律,并提出了一种可行的增强方法。Low-velocity impact compressive damage of 3-D braided ramie fiber reinforced compositesLamei Wang, Baozhong Sun, Ming Cai, Bohong Gudoi:10.1016/j.compstruct.2025.119000三维编织苎麻纤维增强复合材料低速冲击压缩损伤研究Impact damage mechanisms of natural plant fiber reinforced composites are essential for their structural design and practical applications. This study reports quasi-static and dynamic compressive behaviors of three-dimensional braided ramie fiber reinforced composites (3DRFRC) and the comparison with carbon fiber reinforced composites (3DCFRC). The results show that the 3DRFRC has a long yield stage under the quasi-static compression owing to ramie fiber bend. The 3DRFRC exhibits higher in-plane dynamic compressive properties than those of the 3DCFRC, and the energy absorption rate (EAR) of the former is 27 % more than that of the latter at 30 J impact energy. EAR of the four-directional in the 3DRFRC exceeds 90 % under dynamic compression and is higher than that of the five-directional owing to more accessible deformations. The FEA results show that the resin damage in yarn was the leading cause of yarn damage under dynamic compression. The ramie fiber bend and lumen collapse are micro-scale damage mechanisms of the 3DRFRC under in-plane and out-of-plane dynamic compression, respectively.天然植物纤维增强复合材料的冲击损伤机理对其结构设计和实际应用具有重要意义。本文报道了三维编织苎麻纤维增强复合材料(3DRFRC)的准静态和动态压缩性能,并与碳纤维增强复合材料(3DCFRC)进行了比较。结果表明:在苎麻纤维弯曲的准静态压缩作用下,3DRFRC具有较长的屈服阶段;3DRFRC比3DCFRC表现出更高的面内动态压缩性能,在30 J冲击能量时,前者的能量吸收率(EAR)比后者高27 %。动态压缩下,3DRFRC中四向的EAR值超过90% %,由于变形更容易接近,因此高于五向。有限元分析结果表明,在动态压缩条件下,纱线中的树脂损伤是纱线损伤的主要原因。苎麻纤维弯曲和管腔塌陷分别是3DRFRC在面内和面外动态压缩下的微尺度损伤机制。Composites Part A: Applied Science and ManufacturingSuperior multifunctional protecting property of novel slippery integrated thin coating balancing surface and internal designDaowei Lai, Yanfei Ma, Bin Li, Zhenjun Peng, Wufang Yang, Qiangliang Yu, Xiangfei Zhao, Bo Yu, Chufeng Sun, Feng Zhoudoi:10.1016/j.compositesa.2025.108774新型光滑一体化薄涂层平衡表面和内部设计,具有优越的多功能保护性能We developed a novel solid–liquid composite coating with a gradient distribution of liquid-like brush grafting polysilazane and well-distributed modified graphene oxide, integrating anti-corrosion and underwater anti-adhesion properties, which exhibits stale anti-fouling and drag reduction properties. The corrosion current of the coating decreases by six orders of magnitude compared to that of the substrate, and it has an extremely long salt spray lifespan of over 1440 h with the thickness approximately 20 μm. It also achieves over 97 % reduction in microbial contamination, and the maximum drag reduction rate reaches about 36 %, exhibiting outstanding antifouling and drag reduction performance. Impressively, the drag reduction rate remains very stable even after the corrosion test, followed by algae adhesion tests and after abrasion. Even the coating is worn, it can still maintain relatively stable protective performance. This work provides a novel and feasible method for the engineering application of ocean antifouling and drag reduction.我们开发了一种新型的固液复合涂层,该涂层具有梯度分布的液体状电刷接枝聚硅氮烷和均匀分布的改性氧化石墨烯,集防腐和水下抗粘着性能于一体,具有良好的防污和减阻性能。与基材相比,涂层的腐蚀电流减小了6个数量级,且厚度约为20 μm的涂层具有超过1440 h的超长盐雾寿命。微生物污染减少97%以上,最大减阻率达36%左右,具有出色的防污减阻性能。令人印象深刻的是,即使经过腐蚀试验、藻类附着试验和磨损试验,减阻率仍然非常稳定。即使涂层磨损,仍能保持相对稳定的防护性能。为海洋防污减阻的工程应用提供了一种新颖可行的方法。Composites Part B: EngineeringUltra-High Temperature Ceramic (HfC) reinforcement of laser powder-directed energy deposited Inconel 718: Microstructural evolution and tensile properties at room and high temperaturesWonjong Jeong, Joowon Suh, Suk Hoon Kang, Yejin Kang, Minseok Lee, Taegyu Lee, Kang Taek Lee, Ho Jin Ryudoi:10.1016/j.compositesb.2025.112281 激光粉末定向能沉积Inconel 718的超高温陶瓷(HfC)增强:室温和高温下的组织演变和拉伸性能This study explores the influence of ultra-high-temperature ceramic (UHTC) hafnium carbide (HfC) reinforcement on the microstructural evolution and mechanical properties of Inconel 718 produced by laser powder directed energy deposition (LP-DED). Inconel 718 powder was uniformly coated with HfC particles (HfCp) via the surface modification and reinforcement transplantation (SMART) process. The introduction of HfCp, which accumulated at the melt pool surface during LP-DED, significantly enhanced the laser beam absorptivity, inducing localized heating that resulted in the dissolution of HfC and the formation of secondary phases, such as Ni5Hf, (Hf, Nb, Ti)C, and Hf-enriched Laves phases. These secondary phases, causing Nb depletion, contributed to grain refinement, stabilized the microstructure, and promoted the formation of γ′/γ′′ co-precipitates. Mechanical testing revealed that at 650°C, Inconel 718 samples reinforced with 1.5 vol% and 3.0 vol% HfC demonstrated superior tensile strength and elongation compared to the unreinforced sample, with no observed serration behavior. The secondary phases enhanced the dislocation density and strain-hardening behavior, while acting as diffusion barriers to prevent oxidation-induced intergranular cracking, whereas Hf and C specifically stabilized the grain boundaries, further enhancing the oxidation resistance at elevated temperatures. These results underscore the importance of reinforcing the laser beam absorptivity during the fabrication of high-performance composites by LP-DED and confirm that HfC-reinforced Inconel 718 has great potential for high-temperature applications.研究了超高温陶瓷(UHTC)碳化铪(HfC)增强对激光粉末定向能沉积(LP-DED)制备的Inconel 718显微组织演变和力学性能的影响。通过表面改性和增强移植(SMART)工艺,在Inconel 718粉末表面均匀包裹HfC颗粒(HfCp)。在LP-DED过程中,积累在熔池表面的HfCp的引入显著增强了激光束的吸收率,引起局部加热,导致HfC的溶解和二次相的形成,如Ni5Hf, (Hf, Nb, Ti)C和富Hf的Laves相。这些次级相导致Nb损耗,有助于晶粒细化,稳定组织,促进γ′/γ”共析出相的形成。力学测试表明,在650℃时,添加1.5 vol%和3.0 vol% HfC增强的Inconel 718样品的抗拉强度和伸长率优于未增强的样品,没有观察到锯齿现象。二次相提高了位错密度和应变硬化行为,同时作为扩散屏障防止氧化引起的晶间开裂,而Hf和C特别稳定了晶界,进一步增强了高温下的抗氧化性。这些结果强调了在LP-DED制备高性能复合材料过程中增强激光吸收率的重要性,并证实了hfc增强Inconel 718在高温应用方面具有巨大的潜力。Tung oil-derived polyurethane composite foams based on dual dynamic phenol-carbamate exchange with desirable mechanical properties, flame retardancy and recyclabilityBaozheng Zhao, Fei Song, Zheng Pan, Yijiao Xue, Linfeng Tian, Tiancheng Zhang, Li Tan, Rui Yang, Yonghong Zhou, Meng Zhangdoi:10.1016/j.compositesb.2025.112306 基于酚醛-氨基甲酸酯双动态交换的桐油衍生聚氨酯复合泡沫具有良好的力学性能、阻燃性和可回收性At present, thermoset polyurethane foams were mainly derived from petroleum-based resources and faced inherent challenges such as difficulty in recycling and fire hazard. In this study, tung oil and catechol were used to prepare tung oil-derived polyphenols via Friedel-Crafts alkylation reaction. These polyphenols were combined with isocyanate to synthesize tung oil-derived polyurethane (TPU) foam. With the presence of dual dynamically cross-linked phenol-carbamate bonds, the TPU foam could be hot-pressed several times into a smooth and homogeneous TPU film. To improve the fire resistance and compressive strength of TPU foam, phytic acid functionalized metal-organic frameworks (UiO-66-NH2@PA) flame retardants were successfully synthesized by one-pot solvothermal method. By adding 20 wt% of flame retardants, the TPU composite foams achieved a UL-94 V-0 flammability rating with a limiting oxygen index of 28.1 vol%. The total heat release, total smoke release, CO production and CO2 production of the TPU composite foams were reduced by 43.1%, 57.8%, 63.6% and 62.1%, respectively, compared to the pure TPU foam. Furthermore, the compressive strength of the TPU composite foam continued to increase with increasing flame retardants content, reaching a maximum of 0.55 MPa. Importantly, the introduction of the flame retardants didn't affect the hot-press recycling performance of the TPU foam, but instead improved the tensile strength and flame retardancy of the recycled TPU film. This work paved the way to produce bio-based PU foam with excellent flame retardancy and recyclability.目前,热固性聚氨酯泡沫塑料主要来源于石油基资源,面临着回收困难和火灾危险等固有挑战。本研究以桐油和儿茶酚为原料,通过Friedel-Crafts烷基化反应制备桐油衍生多酚。这些多酚与异氰酸酯结合合成桐油衍生聚氨酯(TPU)泡沫。由于双动态交联酚氨基甲酸酯键的存在,TPU泡沫可以多次热压成光滑均匀的TPU膜。为了提高TPU泡沫材料的耐火性和抗压强度,采用一锅溶剂热法制备了植酸功能化金属有机骨架(UiO-66-NH2@PA)阻燃剂。通过添加20 wt%的阻燃剂,TPU复合泡沫达到UL-94 V-0的可燃性等级,极限氧指数为28.1 vol%。与纯TPU泡沫相比,TPU复合泡沫的总放热量、总排烟量、CO产生量和CO2产生量分别降低了43.1%、57.8%、63.6%和62.1%。随着阻燃剂含量的增加,TPU复合泡沫的抗压强度持续增加,最大抗压强度为0.55 MPa。重要的是,阻燃剂的引入不影响TPU泡沫的热压回收性能,反而提高了回收TPU膜的拉伸强度和阻燃性。为制备具有优异阻燃性和可回收性的生物基聚氨酯泡沫塑料铺平了道路。The impact of crystalline PEEK sizing agent on the interfacial crystallization behavior and interfacial properties of carbon fiber reinforced PEEK compositesSiyu Zhong, Zhongxin Dong, Yanwei Xiao, Yuan Li, LiangLiang Pei, Shengdao Wang, Guibin Wangdoi:10.1016/j.compositesb.2025.112307 结晶型PEEK施胶剂对碳纤维增强PEEK复合材料界面结晶行为及界面性能的影响In recent years, numerous studies have reported the application of crystalline sizing agents for the interfacial modification of carbon fiber reinforced polyether ether ketone (PEEK/CF) composites. However, the underlying mechanism by which these agents improve the interfacial properties remains unclear. Therefore, the interfacial enhancement mechanism of PEEK/CF composites using crystalline PEEK sizing agents was explored from a microscopic perspective, specifically focusing on interfacial crystallization in this study. Firstly, the crystallization behavior of PEEK on the CF surfaces modified with varying concentrations of crystalline PEEK sizing agents was investigated using polarized optical microscope (POM). It was observed that the sizing agent could induce the formation of PEEK transcrystallinity (TC) on the CF surface, with the 1 wt% concentration of sizing agent resulting in the densest crystal nuclei. The lamellar morphology and molecular orientation of the TC layers were further analyzed. Correspondingly, higher interfacial shear strength (IFSS) was observed in PEEK/CF composites with denser TC structures. Furthermore, the film tensile tests and chemical solvent erosion experiments were conducted to investigate the distribution of weak interfacial phases. It was found that the TC layer did not introduce new "weak interfacial phases" into the composites and exhibited superior resistance to solvent erosion. Finally, the mechanism of action of crystalline PEEK sizing agents was discussed. It was proposed that PEEK molecules from the sizing agent could effectively fill the voids at the interface of the composites which were caused by the low mobility of high-viscosity PEEK resin matrix. This led to an increase in nucleation sites on the CF surface and the formation of a denser TC layer.近年来,大量研究报道了结晶施胶剂在碳纤维增强聚醚醚酮(PEEK/CF)复合材料界面改性中的应用。然而,这些试剂改善界面性能的潜在机制尚不清楚。因此,本研究从微观角度探讨结晶PEEK施胶剂对PEEK/CF复合材料界面增强机理,重点研究界面结晶作用。首先,利用偏光显微镜(POM)研究了聚醚醚酮在不同浓度聚醚醚酮施胶剂改性的CF表面上的结晶行为。结果表明,施胶剂可诱导聚醚醚酮在CF表面形成跨结晶度(TC),当施胶剂浓度为1wt %时晶核密度最大。进一步分析了TC层的层状形貌和分子取向。相应的,TC结构致密的PEEK/CF复合材料具有更高的界面剪切强度(IFSS)。通过薄膜拉伸试验和化学溶剂侵蚀试验研究了弱界面相的分布。发现TC层没有在复合材料中引入新的“弱界面相”,并且具有较好的抗溶剂侵蚀性能。最后讨论了结晶型PEEK施胶剂的作用机理。研究结果表明,施胶剂中的PEEK分子可以有效填充高粘度PEEK树脂基体低迁移率造成的复合材料界面空隙。这导致CF表面的成核位点增加,形成更致密的TC层。Enhancement of Flexural Strength of γ-C2S Carbonated Compacts through In Situ Synthesis of Mg-calciteYunchao Liang, Yunpeng Liu, Zhichao Liu, Fazhou Wang, Shuguang Hudoi:10.1016/j.compositesb.2025.112331原位合成镁方解石提高γ-C2S碳化压块抗弯强度To address the inherent brittleness of carbonated gamma calcium silicate (γ-C2S) material, we controlled the crystal transformation of γ-C2S during the carbonization process to facilitate the development of Mg-calcite particles as secondary phases. In this study, highly Mg-calcite carbonated compacts were synthesized in situ by modulating the concentration of MgCl2 in an aqueous solution. The mechanisms underlying the toughening of these compacts are discussed in detail. The resulting carbonated compacts prepared in 0.1 or 0.5 mol/L MgCl2 solutions exhibited compressive strengths over 100 MPa and flexural strengths exceeding 40 MPa. Additional MgCl2 introduced a chemical looping that accelerates the carbonation reaction. Simultaneously, the formation of Mg-calcite and aragonite induced structural deformation and internal coherent strain, enhancing the capacity of the γ-C2S carbonated compacts to withstand high flexural stresses. Furthermore, the interaction of Mg2+ ions with silica gels promoted the formation of highly polymerized M-S-H structures, resulting in an increased elastic modulus of the carbonated matrix. This toughening strategy effectively addresses the inherent challenges associated with carbonatable binders and holds promise for developing low-carbon cement alternatives.为了解决碳化γ硅酸钙(γ-C2S)材料固有的脆性问题,我们在碳化过程中控制γ-C2S的晶型转变,促进镁方解石颗粒作为次生相的发育。在本研究中,通过调节水溶液中MgCl2的浓度,原位合成了高镁方解石碳酸化致密物。详细讨论了这些致密材料增韧的机理。在0.1或0.5 mol/L MgCl2溶液中制备的碳化压块抗压强度超过100 MPa,抗折强度超过40 MPa。额外的MgCl2引入了一个化学环,加速了碳化反应。同时,镁方解石和文石的形成引起了结构变形和内部相干应变,增强了γ-C2S碳化压块的高弯曲应力承受能力。此外,Mg2+离子与硅胶的相互作用促进了高度聚合的M-S-H结构的形成,导致碳化基体的弹性模量增加。这种增韧策略有效地解决了与可碳化粘合剂相关的固有挑战,并为开发低碳水泥替代品带来了希望。 来源:复合材料力学仿真Composites FEM

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