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【新文速递】2024年1月6日固体力学SCI期刊最新文章

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今日更新:International Journal of Solids and Structures 5 篇,Journal of the Mechanics and Physics of Solids 1 篇,International Journal of Plasticity 1 篇,Thin-Walled Structures 6 篇

International Journal of Solids and Structures

Analytical solution of multilayered structures with Green’s function

Shouming Shang, Jinxin Xiao, Tianlin Jiang, Wen-Hua Zhang

doi:10.1016/j.ijsolstr.2023.112636

具有格林函数的多层结构的解析解

It is well known that for solving the problem of thin multilayered structures in complex working conditions, the calculation accuracy and efficiency of the finite element method are significantly inferior to those of the analytical solution. However, the prediction of road life requires precise and detailed mechanical performance analysis. To satisfy this requirement, this study first utilized the three-dimensional Green’s function adapted to transversely isotropic multilayered structures with arbitrary thicknesses based on the mirroring image principle. Then, the analytical solution of multilayered pavements subjected to multiple loadings without complex integral or inverse transformations was derived. Furthermore, an equivalent sliding interface model was proposed to simulate the imperfect interface or thin interlayer of multilayered pavements. Numerical examples verified the suitability and accuracy of the analytical solution thorough the comparison with the other theory and experimental results. Moreover, the key factors affecting the performance of pavements, such as the anisotropy and thickness of each layer, loading direction, and pavement friction coefficient, were investigated to provide reliable numerical and theoretical bases for the optimal design of pavement structures.

众所周知,在解决复杂工况下的薄多层结构问题时,有限元法的计算精度和效率明显低于解析法。然而,道路寿命的预测需要精确详细的力学性能分析。为了满足这一要求,本研究首先利用了基于镜像原理的三维格林函数,该函数适用于任意厚度的横向各向同性多层结构。然后,在不进行复杂积分或反变换的情况下,推导出了多层路面在多重荷载作用下的解析解。此外,还提出了一个等效滑动界面模型,用于模拟多层路面的不完美界面或薄夹层。通过与其他理论和实验结果的对比,数值实例验证了分析解决方案的适用性和准确性。此外,还研究了影响路面性能的关键因素,如各层的各向异性和厚度、加载方向和路面摩擦系数等,为路面结构的优化设计提供了可靠的数值和理论依据。


Approximate contact force model for viscoelastic materials based on generalized Maxwell model

Suhang Ding, Yiqun Hu, Bin Jian, Yuhang Zhang, Lei Su, Re Xia, Guoming Hu

doi:10.1016/j.ijsolstr.2024.112645

基于广义麦克斯韦模型的粘弹性材料近似接触力模型

This paper proposes a novel approximate model for estimating the normal contact force between a rigid sphere and a viscoelastic half-space based on the generalized Maxwell model. The relaxation function derived from the generalized Maxwell model is applied to the solution to the elastic contact problem based on the elastic-viscoelastic correspondence to obtain an integral expression of pressure for viscoelastic contact. Using the approximate method on the basis of Taylor series, the integral expression is translated into an explicit function of displacement, velocity, time and material properties. A normal contact force model is established by integrating the pressure over contact area. A relaxation test of Nafion® XL is conducted to capture the viscoelastic parameters, and these parameters are employed to simulate the contact behaviors using the finite element method (FEM) to determine the scale factor in the contact force model. In order to verify the validity of the approximate model, the outcomes obtained from the model are compared with those generated by the FEM. A parametric study is conducted to analyze the effects of variations in parameters on normal contact behaviors. The results indicate that the established model is able to predict the contact responses of the viscoelastic materials with complex mechanical characteristics.

本文基于广义麦克斯韦模型,提出了一种估算刚性球体与粘弹性半空间之间法向接触力的新型近似模型。根据弹性-粘弹性对应关系,将广义麦克斯韦模型导出的松弛函数应用于弹性接触问题的解,从而得到粘弹性接触压力的积分表达式。利用基于泰勒级数的近似方法,将积分表达式转化为位移、速度、时间和材料属性的显式函数。通过对接触面积上的压力进行积分,建立了法向接触力模型。对 Nafion® XL 进行松弛测试以获取粘弹性参数,并利用这些参数通过有限元法(FEM)模拟接触行为,以确定接触力模型中的比例因子。为了验证近似模型的有效性,将模型得出的结果与有限元法得出的结果进行了比较。还进行了参数研究,分析参数变化对正常接触行为的影响。结果表明,所建立的模型能够预测具有复杂机械特性的粘弹性材料的接触响应。


A fully coupled electromagnetic-thermo-mechanical model for honeycomb microwave absorbing structure

Han Yan, Bin Fu, Yimeng Shan, Yungang Sun, Xuefeng Yao

doi:10.1016/j.ijsolstr.2024.112646

蜂窝微波吸收结构的全耦合电磁-热力学模型

Honeycomb microwave absorbing structures typically operate under multiple physical fields, resulting in complex electromagnetic-thermo-mechanical coupling phenomena. In the present work, a multi-physics macroscopic model of the absorbing performance for honeycomb microwave absorption structures is proposed by incorporating the concept of load factor and the transmission line theory. Then, the interactive relationship between electromagnetic-thermo-mechanical coupling fields and the absorbing performance of the structure were thoroughly explored. Furthermore, the evolution law of the load factors under both single-field and multi-field coupling is analyzed and verified. The main originality of the proposed model is its capability to predict the evolution of absorbing performance under electromagnetic-thermo-mechanical coupling loading, which provides valuable theoretical guidance for designing advanced honeycomb microwave absorbing structures.

蜂窝微波吸收结构通常在多个物理场下工作,从而产生复杂的电磁-热力学耦合现象。本研究结合负载因子概念和传输线理论,提出了蜂窝微波吸收结构吸收性能的多物理场宏观模型。然后,深入探讨了电磁-热力学耦合场与结构吸波性能之间的交互关系。此外,还分析并验证了单场耦合和多场耦合下负载因子的演化规律。该模型的主要独创性在于能够预测电磁-热力学耦合载荷下的吸波性能演变,为设计先进的蜂窝微波吸波结构提供了宝贵的理论指导。


Magnetoactive asymmetric mechanical metamaterial for tunable elastic cloaking

Quan Zhang, Gengkai Hu, Stephan Rudykh

doi:10.1016/j.ijsolstr.2024.112648

用于可调弹性隐形的磁活性非对称机械超材料

We propose a magnetic field-induced asymmetric mechanical metamaterial for tunable transformation-based elastic cloaking. The metamaterial is designed by integrating hard-Magnetic Active Elastomers (hMAEs) and combining zero-stress collapse modes to produce a unique asymmetric behavior controlled by an external magnetic field. The relationship bridging the microstructure and the desired cloaking performance is presented. This magneto-metamaterial design is applied to achieve tunable static elastic cloaking. The theoretical predictions, together with the numerical tests under various static loads, demonstrate encouraging cloaking performance. The study also highlights the impact of magneto-mechanical coupling and offers the first remotely-controllable hMAE-based cloaking solution, with promising potential in various applications including stress shielding and stealth technologies.

我们提出了一种磁场诱导的非对称机械超材料,用于基于可调变换的弹性隐形。这种超材料是通过整合硬磁活性弹性体(hMAEs)设计的,并结合了零应力塌缩模式,从而产生了一种由外部磁场控制的独特非对称行为。本文介绍了微结构与所需隐形性能之间的关系。这种磁性超材料设计可用于实现可调静态弹性隐形。理论预测和各种静态负载下的数值测试都证明了令人鼓舞的隐形性能。该研究还强调了磁-机械耦合的影响,并提供了首个可远程控制的基于 hMAE 的隐形解决方案,在包括应力屏蔽和隐形技术在内的各种应用中具有广阔的发展前景。


Non-contact reconstitution of the traction distribution using incomplete deformation measurements: Methodology and Experimental Validation

Yue Mei, Dongmei Zhao, Rongyao Kang, Xinyu Wang, Bo Wang, Dawei Song, Li Dong, Hao Jiang, Stephane Avril

doi:10.1016/j.ijsolstr.2024.112650

利用不完全变形测量对牵引力分布进行非接触式重组:方法与实验验证

Traction distribution is often unknown in solid mechanics. However, identifying traction distribution with both high accuracy and spatial resolution can sometimes be critical. In this paper, we consider the frequent situation where incomplete deformation measurements, such as partial surface measurements obtained by digital image correlation, are available. For such situations, we propose to achieve the complete identification of boundary tractions, using an optimization based inverse method. The feasibility and robustness of the proposed approach are firstly assessed with numerical simulations. We show that complete traction distributions can be identified with high accuracy even when there is noise added to the deformation measurements. More specifically, the relative error was less than 3% even with 10% noise. Moreover, the effect of noise depends significantly on the level of incompleteness of the deformation data. We show for instance that when the measurement area is 8.3% of the solid, the relative error can be 5 times larger than when the measurement area is 33.3%. However, even with 8.3% deformation measurement area of the solid, the relative error of the mapped traction distribution can be less than 6%. Besides, the accuracy of the mapped traction distribution can be further improved if the region of the deformation measurement is closer to the traction boundary. We eventually validate the proposed inverse approach using incomplete experimental datasets consisting in tensile tests carried out on two elastic samples. We obtain very promising results, with relative errors below 4% using the measured displacements of only 3 points, which is promising to open potential applications in different fields of engineering.

在固体力学中,牵引力分布往往是未知的。然而,以高精度和高空间分辨率识别牵引力分布有时至关重要。在本文中,我们考虑了经常出现的不完整变形测量的情况,例如通过数字图像相关性获得的部分表面测量。针对这种情况,我们建议使用基于优化的逆方法来实现边界牵引的完整识别。我们首先通过数值模拟评估了所提方法的可行性和稳健性。我们发现,即使在变形测量中添加了噪声,也能高精度地识别出完整的牵引力分布。更具体地说,即使噪声为 10%,相对误差也小于 3%。此外,噪声的影响很大程度上取决于变形数据的不完整程度。例如,我们发现当测量区域为实体的 8.3% 时,相对误差可能比测量区域为 33.3% 时大 5 倍。然而,即使变形测量面积为实体的 8.3%,绘制的牵引力分布图的相对误差也可小于 6%。此外,如果变形测量区域更靠近牵引边界,则绘制牵引力分布图的精度还能进一步提高。最终,我们利用对两个弹性样本进行拉伸测试的不完整实验数据集验证了所提出的逆方法。我们获得了非常有前景的结果,使用仅 3 个点的测量位移,相对误差低于 4%,这为在不同工程领域的潜在应用带来了希望。


Journal of the Mechanics and Physics of Solids

Thermal fluctuations (eventually) unfold nanoscale origami

Matthew Grasinger, Pradeep Sharma

doi:10.1016/j.jmps.2023.105527

热波动(最终)展开纳米级折纸

Origami is a scale invariant paradigm for morphing robotics, deployable structures (e.g. satellites, disaster relief shelters, medical stents), and metamaterials with tunable thermal, mechanical, or electromagnetic properties. There has been a resurgence of interest in using origami principles–along with 2D materials or DNA–to design a wide array of nanoscale devices. In this work, we take cognizance of the fact that small-scale devices are vulnerable to entropic thermal fluctuations and thus a foundational question underlying small-scale origami pertains to its stability, i.e. the origami structure’s propensity to “unfold” due to thermal fluctuations and the rate at which the unfolding will ensue. To properly understand the behavior of these origami-based nanodevices, we must simultaneously consider the geometric mechanics of origami along with the interplay between thermal fluctuations, entropic repulsive forces, van der Waals attraction, and other molecular-scale phenomena. In this work, to elucidate the rich behavior underpinning the evolution of an origami device at the nanoscale, we develop a minimal statistical mechanics model of folded nanoscale sheets. We use the model to investigate (1) the thermodynamic multistability of nanoscale origami structures and (2) the rate at which thermal fluctuations drive its unfolding–that is, its temporal stability. We identify, for the first time, an entropic torque that is a critical driving force for the unfolding process. Both the thermodynamic multistability and temporal stability have a nontrivial dependence on the origami’s bending stiffness, the radii of curvature of its creases, the ambient temperature, its thickness, and its interfacial energy (between folded layers). Specifically, for graphene, we show that there is a critical side length below which it can no longer be folded with stability; similarly, there exists a critical crease diameter, membrane thickness (e.g. for multilayer graphene), and temperature above which a crease cannot be stably folded. To investigate the rate of thermally driven unfolding, we extend Kramers’ escape rate theory to cases where the minima of the energy well occurs at a boundary. Rates of unfolding are found to span from effectively zero to instantaneous, and there is a clear interplay between temperature, geometry, and mechanical properties on the unfolding rate.

折纸是变形机器人、可部署结构(如卫星、救灾避难所、医疗支架)以及具有可调热、机械或电磁特性的超材料的规模不变范例。人们对利用折纸原理以及二维材料或 DNA 设计各种纳米级设备的兴趣再次升温。在这项研究中,我们认识到小尺度器件容易受到熵热波动的影响,因此小尺度折纸的一个基本问题是其稳定性,即折纸结构由于热波动而 "展开 "的倾向以及展开的速度。要正确理解这些基于折纸的纳米器件的行为,我们必须同时考虑折纸的几何力学以及热波动、熵排斥力、范德华吸引力和其他分子尺度现象之间的相互作用。在这项工作中,为了阐明折纸器件在纳米尺度上演化的丰富行为,我们建立了一个折叠纳米级薄片的最小统计力学模型。我们利用该模型研究了:(1) 纳米级折纸结构的热力学多稳定性;(2) 热波动驱动其展开的速率,即其时间稳定性。我们首次发现了一种熵力矩,它是展开过程的关键驱动力。热力学多稳定性和时间稳定性都与折纸的弯曲刚度、折痕曲率半径、环境温度、厚度和界面能(折叠层之间)有着非同小可的关系。具体来说,对于石墨烯,我们发现存在一个临界边长,低于该边长的折纸无法再稳定折叠;同样,存在一个临界折痕直径、膜厚(例如多层石墨烯)和温度,高于该温度的折痕无法稳定折叠。为了研究热驱动解折的速率,我们将克拉默逃逸率理论扩展到能量井的最小值出现在边界的情况。研究发现,展开率从实际为零到瞬时展开,温度、几何形状和机械特性对展开率的影响是显而易见的。


International Journal of Plasticity

A dislocation-based damage-coupled constitutive model for single crystal superalloy: unveiling the effect of secondary orientation on creep life of circular hole

Zixu Guo, Ziyuan Song, Haohao Liu, Daijun Hu, Dawei Huang, Xiaojun Yan, Wentao Yan

doi:10.1016/j.ijplas.2024.103874

基于位错的单晶超合金损伤耦合构造模型:揭示二次取向对圆孔蠕变寿命的影响

Circular holes in single crystal (SX) turbine blades are susceptible to creep failure at high temperatures, due to the stress concentrations near the holes. In this study, a dislocation-based damage-coupled constitutive model for SX superalloys is developed, validated, and applied to unveil the effect of secondary orientation on the creep life of circular holes. The structure-induced geometrically necessary dislocations (GND) density resulting from the macroscopic strain gradient is incorporated. The dissipated energy is employed as the indicator to predict crack nucleation. Initially, the specimens without a hole are employed to calibrate the parameters and validate the model in the absence of structure-induced GND. Creep experiments incorporating the digital image correlation technique are conducted on the specimens with a hole under different secondary orientations, which aims to validate the simulated strain distribution, crack nucleation location, and creep life under the influence of structure-induced GND. The results indicate that the incorporation of structure-induced GND contributes to mitigating the conservatism in the creep life prediction of circular holes. Because, the GND can enhance dislocation hardening near the hole, extending the predicted life and improving the accuracy of life prediction. Meanwhile, both experiments and simulations indicate that the secondary orientation influences the crack nucleation locations at the hole edge. The variation in the creep life at different secondary orientations is attributed to the changes in both the maximum value and uniformity of resolved shear stresses distributed across slip systems. Finally, the model is applied to simulate the creep behavior of a circular hole under various secondary orientations, stresses, and temperatures. An empirical model is developed to rapidly evaluate the creep life of a circular hole in the SX superalloy, which facilitates the engineering application of the proposed model.

由于单晶(SX)涡轮叶片上的圆孔附近存在应力集中,因此在高温下很容易发生蠕变破坏。本研究针对 SX 超合金开发、验证并应用了基于位错的损伤耦合构成模型,以揭示二次取向对圆孔蠕变寿命的影响。宏观应变梯度导致的结构诱发的几何必要位错(GND)密度被纳入其中。耗散能量被用作预测裂纹成核的指标。起初,采用无孔试样来校准参数,并在无结构诱导 GND 的情况下验证模型。结合数字图像相关技术,在有孔的试样上进行了不同次要方向的蠕变实验,旨在验证结构诱导 GND 影响下的模拟应变分布、裂纹成核位置和蠕变寿命。结果表明,加入结构诱导 GND 有助于减轻圆孔蠕变寿命预测的保守性。因为 GND 可以增强孔附近的位错硬化,延长预测寿命,提高寿命预测的准确性。同时,实验和模拟都表明,二次取向会影响孔边缘的裂纹成核位置。不同次要方向上蠕变寿命的变化归因于分布在滑移系统上的解析剪应力的最大值和均匀性的变化。最后,应用该模型模拟了圆孔在不同次生方向、应力和温度下的蠕变行为。建立的经验模型可快速评估 SX 超级合金圆孔的蠕变寿命,从而促进了所提模型的工程应用。


Thin-Walled Structures

Post-fire behaviour and resistances of square recycled aggregate concrete-filled stainless steel tube stub columns

Ziyi Wang, Yukai Zhong, Ke Jiang, Meini Su, Ou Zhao

doi:10.1016/j.tws.2024.111564

方形再生骨料混凝土填充不锈钢管桩柱的火灾后行为和抗性

Experimental and numerical studies on the cross-section compressive behaviour and residual resistances of square recycled aggregate concrete-filled stainless steel tube (RACFSST) stub columns after exposure to fire are reported in this paper. An experimental programme was firstly carried out on twelve stub column specimens with three recycled coarse aggregate replacement ratios (0%, 35% and 70%) after exposure to the ISO-834 standard fire for 0 min (i.e. at ambient temperature), 15 min, 30 min and 45 min. The test results, including load–end shortening curves, failure loads and failure modes, were presented, with the initial compressive stiffness and confinement effect analysed. The experimental programme was followed by a numerical modelling programme, where thermal and mechanical finite element models were developed and validated against the test results and afterwards used to conduct parametric studies to generate additional numerical data over a wide range of cross-section dimensions. Based on the test and numerical data, the relevant design rules for square natural aggregate concrete-filled carbon steel tube stub columns at ambient temperature, as specified in the European code, Australia/New Zealand standard and American specification, were evaluated, using post-fire material properties, for their applicability to square RACFSST stub columns after exposure to fire. The evaluation results generally revealed that the European code and Australian/New Zealand standard led to a good level of design accuracy, while the American specification resulted in slightly conservative post-fire cross-section compression resistance predictions.

本文报告了对方形再生骨料混凝土填充不锈钢管(RACFSST)短柱在遭受火灾后的截面抗压行为和残余阻力的实验和数值研究。首先,对 12 个具有三种再生粗骨料替代率(0%、35% 和 70%)的短柱试样进行了试验,这些试样在 ISO-834 标准火灾中暴露了 0 分钟(即在环境温度下)、15 分钟、30 分钟和 45 分钟。试验结果包括荷载端缩短曲线、破坏荷载和破坏模式,并分析了初始压缩刚度和约束效应。实验计划之后是数值建模计划,根据测试结果开发和验证了热和机械有限元模型,之后用于开展参数研究,以生成更多横截面尺寸范围的数值数据。根据测试和数值数据,对欧洲规范、澳大利亚/新西兰标准和美国规范中规定的环境温度下方形天然骨料混凝土填充碳钢管桩柱的相关设计规则进行了评估,使用了火灾后材料特性,以确定其是否适用于火灾后的方形 RACFSST 桩柱。评估结果普遍表明,欧洲规范和澳大利亚/新西兰标准的设计精确度较高,而美国规范对火灾后截面抗压性的预测略显保守。


Compression performance of 3D-printed thermoplastic auxetic structures

Pan He, Siwen Wang, Miaomiao Zhang, Lin Sang, Liyong Tong, Wenbin Hou

doi:10.1016/j.tws.2024.111558

三维打印热塑性辅助结构的压缩性能

The influence of lattice structural design on the mechanical property has been abundantly investigated, however, the effect of material on the load-carrying performance and energy absorption was seldom studied. In the current work, the auxetic structures fabricated using four materials including polyamide (PA), carbon fiber (CF) reinforced PA (PA/CF), polyether ether ketone (PEEK) and PEEK/CF were 3D-printed, and the compression performance and deformation behavior were compared and explored. The results showed that the deformation mode of auxetic structure were similar, which was not dependent on the material type. However, the compressive strength and modulus of the auxetic structure showed strong dependence on the material properties. Besides, PA and PA/CF auxetic structures displayed better rebound behavior after compression, which was perhaps attributed to the good resilience of PA resin. Therefore, mathematical equations were utilized to predict the compressive property based on the material parameters, showing a good agreement. On the other hand, the simulation of compression process was established and conducted, which confirmed the deformation process as experimental presented. The rebound behavior was further predicted by a loading-releasing cycle with different compression strains. Accordingly, the compression parameters showed great relations with material parameters but little effect on the deformation behavior.

格子结构设计对力学性能的影响已得到大量研究,但材料对承载性能和能量吸收的影响却鲜有研究。本研究采用聚酰胺(PA)、碳纤维(CF)增强 PA(PA/CF)、聚醚醚酮(PEEK)和 PEEK/CF 四种材料制作了 3D 打印辅助结构,并对其压缩性能和变形行为进行了比较和探讨。结果表明,辅助结构的变形模式相似,与材料类型无关。然而,辅助结构的抗压强度和模量与材料特性有很大关系。此外,PA 和 PA/CF 辅助结构在压缩后显示出更好的回弹特性,这可能与 PA 树脂的良好回弹性有关。因此,根据材料参数利用数学方程预测了压缩性能,结果显示两者吻合良好。另一方面,建立并进行了压缩过程模拟,证实了与实验结果一致的变形过程。通过不同压缩应变的加载-释放循环,进一步预测了回弹行为。因此,压缩参数与材料参数关系密切,但对变形行为影响不大。


Real-time hybrid model test to replicate high-rise building resonant vibration under wind loads

Zhou Huimeng, Shao Xiaoyun, Zhang Jianwen, Yao Hongcan, Liu Yanhui, Tan pin, Chen Yangyang, Xu Li, Zhang Yin, Gong Wei

doi:10.1016/j.tws.2024.111559

在风荷载作用下复 制高层建筑共振的实时混合模型试验

In May 2021, the 72-story Shenzhen Saige building experienced abnormal vibration that was strongly felt on many floors and triggered social panic. The tower was therefore closed for more than 2 months resulting in huge economic losses. A preliminary study consisting of field resonant excitation tests and a series of numerical simulations were carried out. It was concluded that the wind loads provoked the higher modes of the building vibration. Specifically, the vibration of the mast, which is located at the building top, induced this abnormal vibration. To validate this conclusion, real-time hybrid model (RTHM) tests was developed to reproduce this building vibration incident. This paper presents the details of the validation RTHM tests including testing design and result discussions. Structural vibration parameters obtained from the field tests were used in the numerical substructure building model, and the experimental substructures were the two scaled down mast models (the cantilever beam section of the masts). During RTHM test, the restoring force of the experimental substructure due to real wind loads induced by an air fan was measured and used in the numerical simulation to compute interface motions. A shaking table was then used to impose the interface motion back to the bottom of the mast model to reproduce the abnormal vibration incident. The demonstrated ability of the developed RTHM testing method to reproduce the resonant phenomenon of the wind-induced tower vibration provides an alternative experimental method to study vibration responses of high-rise buildings in future.

2021 年 5 月,72 层高的深圳赛格大厦发生异常振动,许多楼层都有强烈震感,引发了社会恐慌。赛格大厦因此关闭了两个多月,造成了巨大的经济损失。初步研究包括现场共振激振试验和一系列数值模拟。研究得出的结论是,风荷载引发了建筑物的高频振动模式。具体来说,位于建筑物顶部的桅杆的振动引发了这种异常振动。为了验证这一结论,开发了实时混合模型(RTHM)测试来重现这一建筑振动事件。本文介绍了验证 RTHM 试验的细节,包括试验设计和结果讨论。从现场测试中获得的结构振动参数被用于下层建筑的数值模型,而实验下层建筑则是两个按比例缩小的桅杆模型(桅杆的悬臂梁部分)。在 RTHM 试验期间,测量了实验下部结构在风扇引起的实际风荷载作用下的恢复力,并将其用于数值模拟,以计算界面运动。然后使用振动台将界面运动施加回桅杆模型底部,以重现异常振动事件。所开发的 RTHM 测试方法能够再现风引起的塔楼振动的共振现象,为今后研究高层建筑的振动响应提供了另一种实验方法。


Non-linear stability of isotropic stiffened composite channels under compression

Andrzej Teter, Zbigniew Kolakowski

doi:10.1016/j.tws.2024.111560

压缩条件下各向同性加劲复合材料通道的非线性稳定性

In this study, compressed laminated channels with isotropic stiffeners on their free longitudinal edges are investigated. The use of edge stiffeners in the form of clamps or angles made of an isotropic material significantly affects the behaviour of the structures under study. Two cases of laminate layup are examined, assuming that the columns are freely supported. It is assumed that there are strong interactions between the eigenmodes. In addition to that, in the two analysed cases, the lowest eigenmode is local and does not cause structural failure. Thus, the expected ultimate load-carrying capacity values will be greater than the lowest eigenmode. The perturbation method and the finite element method are employed to solve an eigenproblem and a problem of nonlinear stability loss. The adequacy of the models and boundary conditions used in both methods is validated by comparing local, global, symmetric and antisymmetric as well as distortional eigenmodes. Postbuckling equilibrium paths and ultimate load-carrying capacity values are determined for all analysed cases. In the perturbation analysis, results obtained with the 4- and 5-mode approaches are compared for low pre-deflection amplitudes. Results obtained by all methods showed a very high qualitative agreement. The geometric imperfections used in numerical simulations were assumed to be identical to the eigenmodes with low amplitudes. The FEM results show that this has no effect on the postbuckling equilibrium paths and ultimate load-carrying capacity of the columns. A low amplitude value is enough to disturb the lowest eigenmode.

本研究对在自由纵向边缘使用各向同性加劲件的压缩层叠槽进行了研究。使用夹具或各向同性材料制成的角钢等形式的边缘加劲件会对所研究结构的性能产生显著影响。假设柱子是自由支撑的,研究了两种层压板铺设情况。假设特征模态之间存在强烈的相互作用。此外,在分析的两种情况中,最低特征模态是局部的,不会导致结构破坏。因此,预期的极限承载能力值将大于最低特征模态。采用扰动法和有限元法来解决特征问题和非线性稳定性损失问题。通过比较局部、全局、对称和非对称以及畸变特征模,验证了这两种方法所使用的模型和边界条件的适当性。确定了所有分析案例的屈曲后平衡路径和极限承载能力值。在扰动分析中,对低预偏转振幅时采用 4 模和 5 模方法得出的结果进行了比较。所有方法得出的结果在质量上具有很高的一致性。数值模拟中使用的几何缺陷被假定为与低振幅的特征模态相同。有限元结果表明,这对柱子的屈曲后平衡路径和极限承载能力没有影响。低振幅值足以干扰最低特征模态。


Improved semi-analytical solution for longitudinal mechanical response of tunnels crossing active faults considering nonlinear soil-tunnel interactions and shear effects

Henghong Yang, Mingnian Wang, Xiao Zhang, Li Yu

doi:10.1016/j.tws.2024.111561

考虑非线性土壤-隧道相互作用和剪切效应的穿越活动断层隧道纵向机械响应的改进型半解析解法

Tunnels crossing active faults are susceptible to severe damage. This study establishes an improved semi-analytical methodology for analyzing the mechanical responses of tunnels subjected to active fault dislocation. The methodology incorporates nonlinear axial, transverse, and vertical soil-tunnel interactions, shear effects, and geometric nonlinearity within its governing equations. Compared with existing methods, the proposed method has a significantly extended application range with improved accuracy, and the solution procedure demonstrates exceptional computational efficiency, with each case typically being solved in less than 1 s. The proposed methodology demonstrates outstanding qualitative and quantitative agreement with 3D FEM results across various fault types, as well as with the results obtained from the model test. Additionally, neglecting shear effects results in approximately 1.11 to 1.20 times higher bending moments and 1.13 to 1.19 times higher shear forces of the tunnel. Finally, a parametric analysis was conducted based on the proposed methodology to investigate the influence of critical parameters, such as fault displacement, buried depth, tunnel diameter, soil cohesion, and soil friction angle, on the tunnel response under fault dislocation. The results suggest that the tunnel responses positively correlate with the fault displacement, buried depth, and soil cohesion. Increasing the fault displacement amplifies the vertical shear force and bending moment asymmetry while increasing buried depth reduces this asymmetry. An increase in the tunnel diameter and soil friction angle is associated with a decrease in the peak axial force and an increase in the vertical shear force and bending moment. Additionally, variations in the friction angle do not exert a significant effect on the transverse shear force and bending moment.

穿越活动断层的隧道容易受到严重破坏。本研究建立了一种改进的半分析方法,用于分析受活动断层错动影响的隧道的机械响应。该方法将非线性轴向、横向和竖向土壤-隧道相互作用、剪切效应和几何非线性纳入其控制方程。与现有方法相比,该方法的应用范围大大扩展,精度也有所提高,而且求解过程具有极高的计算效率,通常每个案例的求解时间不超过 1 秒。此外,忽略剪切效应会导致隧道弯矩增加约 1.11 至 1.20 倍,剪力增加约 1.13 至 1.19 倍。最后,根据所提出的方法进行了参数分析,以研究断层位移、埋深、隧道直径、土壤内聚力和土壤摩擦角等关键参数对断层错动下隧道响应的影响。结果表明,隧道响应与断层位移、埋深和土壤内聚力呈正相关。增加断层位移会放大垂直剪力和弯矩的不对称,而增加埋深则会减小这种不对称。隧道直径和土壤摩擦角的增大与轴向力峰值的减小以及垂直剪切力和弯矩的增大有关。此外,摩擦角的变化对横向剪力和弯矩的影响不大。


Seismic behavior of a novel liftable connection for modular steel buildings: Experimental and numerical studies

En-Feng Deng, Yu-Han Wang, Liang Zong, Zhe Zhang, Jun-Feng Zhang

doi:10.1016/j.tws.2024.111563

模块化钢结构建筑新型可升降连接件的抗震性能:实验和数值研究

Modular steel buildings (MSBs) have achieved considerable popularity in multi-to-high rise constructions due to the favorable mechanical characteristic, eco-friendliness, cost-effectiveness, and enhanced construction efficiency. As the critical part of MSBs, the inter-module connection has an important influence on determining the seismic performance of MSBs. This study presented an experimental-numerical investigation on an innovative fully prefabricated liftable connection (FPLC) for MSBs. To study the seismic performance of the FPLC, quasi-static tests were conducted on four full-scale specimens. The seismic behavior of the specimens, including failure mode, hysteretic response, strength and stiffness degradation, deformation characteristic, etc. was evaluated and compared in detail. The effect of the section of the twin-beams, the dog-bone weakening of the beam and the connecting method between the corner fitting and twin-beams on the seismic behavior of the FPLC was revealed. Moreover, the feasibility for seismic application of the FPLC was evaluated according to Chinese code GB 50011-2010 and Eurocode 3 Part 1-8. The results indicated that the proposed FPLC met the limit of elastic and elastic-plastic inter-story drift ratios required by GB 50011-2010. According to Eurocode 3 Part 1-8, the FPLC with welded beams should be classified as “semi-rigid” connections, while the FPLC, whose beams were connected to the column walls by the steel angles and bolts, was classified as a “pinned” connection. Then, a refined finite element model (FEM) was developed and verified by the test results. Furthermore, the verified FEM was utilized to analyze the distribution of the equivalent plastic strain, the stress variation path, and the yielding area of the twin-beams to further reveal the energy dissipation and damage mechanism of the FPLC. Finally, a simplified FEM was established and the comparison with the test results proved its reliability and efficiency. The present study will contribute to provide a comprehensive understanding on seismic performance and design of the inter-module connection for MSBs.

模块化钢结构建筑(MSB)因其良好的力学性能、环保性、成本效益和更高的施工效率,在多高层建筑中得到了广泛的应用。作为 MSB 的关键部分,模块间连接对决定 MSB 的抗震性能具有重要影响。本研究对用于 MSB 的创新型全预制可升降连接(FPLC)进行了实验-数值研究。为了研究 FPLC 的抗震性能,对四个全尺寸试件进行了准静力试验。详细评估和比较了试件的地震行为,包括破坏模式、滞后响应、强度和刚度退化、变形特征等。研究揭示了双梁截面、梁的狗骨削弱以及角配件与双梁之间的连接方式对 FPLC 地震行为的影响。此外,还根据中国规范 GB 50011-2010 和欧洲规范 3 第 1-8 部分评估了 FPLC 抗震应用的可行性。结果表明,拟议的 FPLC 符合 GB 50011-2010 所要求的弹性和弹塑性层间漂移比限值。根据欧洲规范 3 第 1-8 部分,采用焊接梁的 FPLC 应归类为 "半刚性 "连接,而采用角钢和螺栓将梁与柱壁连接的 FPLC 则归类为 "销钉 "连接。然后,开发了改进的有限元模型(FEM),并通过测试结果进行了验证。此外,还利用验证后的有限元模型分析了双梁的等效塑性应变分布、应力变化路径和屈服区域,进一步揭示了 FPLC 的能量耗散和损坏机制。最后,建立了简化有限元模型,并通过与试验结果的对比证明了其可靠性和高效性。本研究将有助于全面了解 MSB 的抗震性能和模块间连接设计。




来源:复合材料力学仿真Composites FEM
ACTMechanicalMaxwellSystemMAGNET振动复合材料非线性建筑焊接裂纹理论材料机器人控制试验PLC螺栓
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【新文速递】2024年1月11日复合材料SCI期刊最新文章

今日更新:Composite Structures 1 篇,Composites Part A: Applied Science and Manufacturing 2 篇,Composites Part B: Engineering 5 篇,Composites Science and Technology 2 篇Composite StructuresA NOVEL DESIGN MODEL FOR PREDICTING THE SHEAR RESISTANCE OF REINFORCED CONCRETE BEAMS STRENGTHENED WITH EBR-CFRP SYSTEMSAmirhossein Mohammadi, Joaquim A.O. Barros, Jose Sena-Cruzdoi:10.1016/j.compstruct.2024.117901预测采用 EBR-CFRP 系统加固的钢筋混凝土梁抗剪性能的新型设计模型Shear resistance prediction of reinforced concrete (RC) beams strengthened with externally bonded reinforcements (EBR) is a challenging task due to the complex nature of shear resisting mechanisms and their intricate interaction. Existing design models often overlook these dependencies, leading to significant variations in prediction accuracy. 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The Fourier-Transform Misalignment Analysis (FTMA) algorithm is able to measure the average alignment of features over an area, and is therefore well-suited to measuring fibre alignment in low-magnification images. In images with few pixels, the precision of the FTMA algorithm depends on the alignment of the image features. Features at 45° can be measured with greater precision than those near 0 or ±90°. To combat this, a new FTMA-MultiRotate method is proposed. This modified algorithm has been assessed against computer-generated images, where it is able to achieve an average accuracy within ±0.5°. It has then further been applied to measure fibre alignment in low-magnification photographs of glass fabrics, and these measurements have been verified against measurements taken manually. 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Active infrared thermography (AIRT) is a fast and cost-efficient NDT technique for inspecting FRP composites. However, this method is easily affected by factors such as inhomogeneous heating, leading to a low level of visualization of defects. To address this issue, this study proposes a novel method called one-dimensional deep convolutional autoencoder active infrared thermography (1D-DCAE-AIRT) to enhance the visualization of internal defects in FRP composites. This method first preprocesses the thermal image sequence acquired by AIRT inspections. Subsequently, high-level thermal features at the pixel level are extracted from the aforementioned preprocessed thermal image sequence using a designed one-dimensional deep convolutional autoencoder (1D-DCAE) model. Finally, the extracted high-level thermal features are employed to generate enhanced visualization results that exhibit improved defect visibility. The results of three kinds of AIRT (eddy current pulsed thermography, flash thermography, and vibrothermography) experiments on FRP composite specimens with artificially introduced defects show that 1D-DCAE-AIRT can effectively enhance the visualization of internal defects. The enhancement effect is better than the conventional techniques of fast Fourier transform (FFT), principal component analysis (PCA), independent component analysis (ICA), and partial least-squares regression (PLSR).纤维增强聚合物(FRP)复合材料已广泛应用于不同的工业领域,因此有必要采用无损检测(NDT)方法来确保结构的完整性和安全性。主动红外热成像(AIRT)是一种用于检测玻璃纤维增强塑料复合材料的快速、经济的无损检测技术。然而,这种方法很容易受到加热不均匀等因素的影响,导致缺陷的可视化程度较低。针对这一问题,本研究提出了一种名为一维深度卷积自动编码器主动红外热成像(1D-DCAE-AIRT)的新方法,以提高玻璃钢复合材料内部缺陷的可视化程度。该方法首先对 AIRT 检测获得的热图像序列进行预处理。然后,使用设计的一维深度卷积自动编码器(1D-DCAE)模型从上述预处理的热图像序列中提取像素级的高级热特征。最后,利用提取的高级热特征生成增强的可视化结果,从而提高缺陷的可见性。在人为引入缺陷的玻璃钢复合材料试样上进行的三种 AIRT(涡流脉冲热成像、闪光热成像和振动热成像)实验结果表明,1D-DCAE-AIRT 能有效增强内部缺陷的可视化。其增强效果优于快速傅立叶变换 (FFT)、主成分分析 (PCA)、独立成分分析 (ICA) 和偏最小二乘回归 (PLSR) 等传统技术。A novel thermoplastic water-soluble sizing agent for the interfacial enhancement of carbon fiber/polyether ether ketone compositesFei Yan, Tianwen Yan, Gaosong Wang, Gang Li, Shengtao Dai, Yuhui Ao, Jintang Duan, Liu Liudoi:10.1016/j.compositesb.2024.111205用于增强碳纤维/聚醚醚酮复合材料界面性能的新型热塑性水溶性施胶剂Recently reported novel water-soluble polyether ether ketone (PEEK) derivative sizing agents have garnered considerable attention for improving interfacial bonding of carbon fiber-reinforced PEEK (CF/PEEK) composites. However, their extensive application is somewhat limited due to two drawbacks: the use of hazardous organic solvents in production and the retention of emulsifiers in sizing dispersion systems. Herein, an extremely hydrophilic sulfonated PEEK with a cardo group (S-PEEK-WC) was synthesized and used to prepare a water-soluble sizing agent. The S-PEEK-WC exhibits excellent thermal stability, with a 5 % decomposition temperature of 446.5 °C, and its aqueous solution remains stable for over six months. A robust interphase was also constructed in the CF/PEEK composites through multiple physicochemical interactions. Compared with the de-sized CF/PEEK composites, the interlaminar shear strength, flexural strength and interfacial shear strength of the CF2/PEEK composites improved by 57.9 %, 56.3 % and 44.8 %, respectively. This approach may shed some light on the development of a valid and environmentally friendly method for preparing water-soluble sizing agents of polyaryletherketone.最近报道的新型水溶性聚醚醚酮(PEEK)衍生物施胶剂在改善碳纤维增强聚醚醚酮(CF/PEEK)复合材料的界面粘合方面引起了广泛关注。然而,由于在生产过程中使用有害的有机溶剂以及在施胶分散体系中保留乳化剂这两个缺点,它们的广泛应用受到了一定的限制。在此,我们合成了一种带有 Cardo 基团的极亲水性磺化聚醚醚酮(S-PEEK-WC),并将其用于制备水溶性施胶剂。S-PEEK-WC 具有出色的热稳定性,5%分解温度为 446.5 °C,其水溶液可保持稳定 6 个月以上。通过多种物理化学相互作用,CF/PEEK 复合材料中还形成了坚固的相间结构。与去尺寸的 CF/PEEK 复合材料相比,CF2/PEEK 复合材料的层间剪切强度、弯曲强度和界面剪切强度分别提高了 57.9%、56.3% 和 44.8%。这种方法有助于开发一种有效且环保的聚芳醚酮水溶性施胶剂制备方法。Full-field characterizations of additively manufactured composite cellular structuresAnil Singh, Behrad Koohbor, George Youssefdoi:10.1016/j.compositesb.2024.111208增材制造复合蜂窝结构的全场特性分析Honeycomb structures possess unique mechanical and structural behaviors, including high specific strength, superior energy absorption, and potential for multifunctionality. The advantages of such structures are bolstered by their realization through additive manufacturing, enabling cellular geometries beyond traditionally fabricated hexagons and facilitating a pathway for hybridization using composite materials to tune the response. This research synthesized photocurable particulate-reinforced resins using mechanically compliant matrix and glass microballoons reinforcement. The modified resins were used to additively manufacture lattice structures with circular and hexagonal unit cell geometries at different glass microballoons reinforcement weight ratios, ranging from neat to 20 wt%. The 3D printed structures were tested under quasi-static and impact loading scenarios to elucidate the interrelationships between the cell geometry, induced deformations, and strain rates. The mechanical testing was coupled with digital image correlation (DIC) to reveal the deformation-geometry interrelationship on the global (macroscale) and local (mesoscale) levels. The multiscale analyses allowed for extensive characterization of the effect of cell geometry and increased weight reinforcement on the mechanical response at a global, sub-cellular, and cellular level, i.e., elucidating the hierarchical dependency. The novelty leading to the current study stems from probing and revealing the deformation state of cellular structures subjected to two loading scenarios using DIC. This study intended to provide mechanistic insights for engineering lattice structures for impact mitigation applications by offering a viable approach to additive manufacturing composite materials.蜂窝结构具有独特的机械和结构特性,包括高比强度、卓越的能量吸收能力和多功能潜力。通过增材制造技术实现蜂窝状几何形状,超越了传统的六边形制造工艺,并为使用复合材料调整响应的混合途径提供了便利,从而增强了此类结构的优势。这项研究利用机械顺应性基体和玻璃微球增强材料合成了光固化微粒增强树脂。改性树脂用于以不同的玻璃微球增强重量比(从未加工到 20 wt%)添加制造具有圆形和六边形单元格几何形状的晶格结构。在准静态和冲击加载情况下对 3D 打印结构进行了测试,以阐明晶胞几何形状、诱导变形和应变率之间的相互关系。机械测试与数字图像相关性(DIC)相结合,揭示了全局(宏观尺度)和局部(中观尺度)层面的变形-几何相互关系。通过多尺度分析,可以从全局、亚细胞和细胞层面广泛描述细胞几何形状和增重加固对机械响应的影响,即阐明分层依赖关系。本研究的新颖之处在于利用 DIC 探测和揭示了细胞结构在两种加载情况下的变形状态。这项研究旨在为工程晶格结构的冲击缓解应用提供机理见解,为增材制造复合材料提供一种可行的方法。‘Resin welding’: A novel route to joining acrylic composite components at room temperatureMachar Devine, Ankur Bajpai, Conchúr M. Ó Brádaigh, Dipa Raydoi:10.1016/j.compositesb.2024.111212树脂焊接":在室温下连接丙烯酸复合材料部件的新方法The solubility of acrylic polymer in its own liquid monomer creates the opportunity to ‘weld’ acrylic-matrix (Elium®) composites without the application of heat. In this method, termed resin welding, acrylic monomeric resin is infused between acrylic-matrix composite parts. The resin dissolves and diffuses into the acrylic matrix and creates a continuous material, and a strong bond, when it polymerises, without the sensitivities of traditional welding methods to adherend or bondline thickness. Single lap shear testing was conducted on resin-welded and adhesively-bonded coupons with varying bondline thicknesses and filling fibres, and the bonding and fracture mechanisms were investigated using SEM and the diffusion of dyed acrylic resin. The highest bond strength of resin-welded coupons reached 27.9 MPa, which is 24 % higher than the strongest weld reported in the literature, indicating that resin welding is a promising alternative to traditional bonding and welding methods for acrylic-matrix composites.丙烯酸聚合物在自身液态单体中的溶解性为无需加热即可 "焊接 "丙烯酸基质 (Elium®) 复合材料创造了机会。在这种称为树脂焊接的方法中,丙烯酸单体树脂被注入丙烯酸基复合材料部件之间。树脂溶解并扩散到丙烯酸基体中,聚合后形成连续的材料和牢固的粘合,而不会像传统焊接方法那样对粘合剂或粘合线厚度产生影响。对具有不同粘合剂厚度和填充纤维的树脂焊接和粘合剂粘合试样进行了单搭接剪切测试,并利用扫描电镜和染色丙烯酸树脂的扩散研究了粘合和断裂机制。树脂焊接试样的最高粘接强度达到 27.9 兆帕,比文献报道的最强焊缝高出 24%,表明树脂焊接是丙烯酸基复合材料传统粘接和焊接方法的一种很有前途的替代方法。Investigation on moisture absorption behavior on GFRP and neat epoxy systems in hygrothermal salt fog agingGeovane de Almeida Santos da Silva, José Roberto Moraes d’Almeida, Daniel Carlos Taissum Cardosodoi:10.1016/j.compositesb.2024.111214研究湿热盐雾老化过程中 GFRP 和纯环氧系统的吸湿行为This work investigates the moisture absorption behavior in epoxy matrix composites reinforced with glass fibers, used in repairs of offshore topside metal pipelines exposed to aging in saline environment. The materials used were a bicomponent DGEBA epoxy and a woven bidirectional E-glass fabric. In order to simulate the harsh environment, the composites were exposed to accelerated hygrothermal aging tests in three independent salt spray chambers at temperatures of 35, 55 and 70 °C and the materials had their mass gain monitored. The moisture absorption of the neat epoxy resin was also investigated and correlated with that of the composites. Thermal analyses by Differential Scanning Calorimetry (DSC) and Dynamic Mechanical Thermal Analysis (DMTA) were performed to evaluate the curing state of the polymeric materials tested and the effects of temperature on the material's post-curing. Fourier-Transform Infrared (FTIR) analyses were performed to investigate the occurrence of post-curing, hydrolysis and thermo-oxidation processes during aging. As expected, it was seen that temperature increased diffusivity for both the composite and the unreinforced epoxy matrix. The neat epoxy resin presented a decrease in moisture absorbed with temperature, evidencing the effect of post-curing on moisture absorption. Furthermore, from the thermal analyses, it was observed the presence of an interphase between matrix and fibers with a Tg higher than the bulk matrix. Non-Fickian models confirmed structural changes caused by temperature and moisture in the materials. A modification of the Berens-Hopfenberg (BH) non-Fickian model was proposed to account for post-curing effects on moisture absorption.这项研究调查了玻璃纤维增强环氧基复合材料的吸湿行为,该复合材料用于修复暴露在盐碱环境中老化的近海上层金属管道。所用材料为双组分 DGEBA 环氧树脂和双向 E 型玻璃纤维编织物。为了模拟恶劣的环境,复合材料在 35、55 和 70 °C 三个独立盐雾箱中进行了加速湿热老化试验,并对材料的增重进行了监测。此外,还研究了纯环氧树脂的吸湿性,并将其与复合材料的吸湿性进行了对比。通过差示扫描量热法(DSC)和动态机械热分析法(DMTA)进行了热分析,以评估受测聚合物材料的固化状态以及温度对材料后固化的影响。傅立叶变换红外(FTIR)分析用于研究老化过程中发生的后固化、水解和热氧化过程。不出所料,复合材料和未增强环氧基质的扩散率都会增加。纯环氧树脂的吸湿率随温度升高而降低,这证明了后固化对吸湿率的影响。此外,从热分析中还观察到基体和纤维之间存在一个间相,其 Tg 高于块状基体。非菲克模型证实了温度和湿气在材料中引起的结构变化。对贝伦斯-霍普芬伯格(BH)非费克模型进行了修改,以考虑固化后对吸湿性的影响。Composites Science and TechnologyEfficient electromagnetic wave absorption of polypyrrole/low-reduction graphene oxide composites through dielectric properties modulationHuan Zhang, Nian Luo, Tinglong Liu, Yu Wang, Feng Chen, Qiang Fudoi:10.1016/j.compscitech.2024.110436 通过介电性能调制实现聚吡咯/低还原氧化石墨烯复合材料的高效电磁波吸收Graphene oxide (GO) is widely used in electromagnetic microwave absorption (EMA) materials due to its abundant oxygen-containing functional groups and defects. Its conductivity, surface functional groups and defect density can be modified by controlling reduction degree to modulate its electromagnetic properties. However, the thermal reduction temperature needed is often too high, exceeding the Curie temperature of magnetic materials, which makes further compounding difficult. Polypyrrole (PPy), as a conductive polymer with high electrical conductivity, is widely used in EMA field and can help regulate the dielectric properties of materials. In this paper, a series of PPy/GO composites with different ratios and reduction degrees were prepared by in situ polymerization and thermal reduction, and their EMA properties were investigated. At a loading amount of 7.5 wt%, the maximum reflection loss of PPy/rGO composites can reach −66.64 dB, and the effective absorption bandwidth can reach 6.74 GHz with a reduction temperature of only 400 °C. Furthermore, the unreduced sample also has excellent absorption performance, which has a wide range of applications for future one-step compositing with magnetic materials in low reduction temperature.氧化石墨烯(GO)因其丰富的含氧官能团和缺陷而被广泛应用于电磁微波吸收(EMA)材料。通过控制还原度可以改变石墨烯的导电性、表面官能团和缺陷密度,从而调节其电磁特性。然而,所需的热还原温度往往过高,超过了磁性材料的居里温度,这给进一步的复合带来了困难。聚吡咯(PPy)作为一种导电性聚合物,具有很高的导电性,被广泛应用于 EMA 领域,有助于调节材料的介电性能。本文通过原位聚合和热还原的方法制备了一系列不同配比和还原度的 PPy/GO 复合材料,并对其 EMA 性能进行了研究。在负载量为 7.5 wt% 时,PPy/rGO 复合材料的最大反射损耗可达 -66.64 dB,有效吸收带宽可达 6.74 GHz,还原温度仅为 400 ℃。此外,未还原样品也具有优异的吸收性能,这对于未来在低还原温度下与磁性材料一步复合具有广泛的应用前景。Thermo-oxidative aging induced multi-scale shrinkages and damages in 3D angle-interlock woven compositesYanan Ke, Shuwei Huang, Baozhong Sun, Frank Ko, Bohong Gudoi:10.1016/j.compscitech.2024.110438 三维角交错编织复合材料的热氧化老化诱导多尺度收缩和损伤The deterioration of resin and interface in composites deteriorate during high-temperature service, would impact both the thermal stability and overall performance significantly. This paper focused on the experimental characterization of multi-scale damage and resin shrinkage within composites induced by thermo-oxidative aging using Micro-CT, SEM and Confocal Interferometric Microscopy (CIM), and exploring the coupling mechanism between them. The results show that damage distribution and propagation are affected by the hierarchical structure of 3-D angle-interlock fabric. Macro-CIM shows that maximum resin shrinkage depth depends on the resin width and aging time. Resin shrinkage profile evolution demonstrated the accelerating effect of resin crack on shrinkage. Micro-CIM shows that macro yarn cracks form through the accumulation of micro resin cracks in resin-rich areas and fiber/resin interface debonding. The formation of fiber/resin interface crack is tied to the resin shrinkage state, only occurring when the surrounding resin shrinkage slope exceeds a specific threshold value.在高温服役期间,复合材料中树脂和界面的劣化会严重影响其热稳定性和整体性能。本文重点利用显微 CT、扫描电镜和共聚焦干涉显微镜(CIM)对热氧化老化诱导的复合材料内部多尺度损伤和树脂收缩进行了实验表征,并探讨了它们之间的耦合机制。结果表明,损伤分布和传播受三维角交错织物分层结构的影响。宏观 CIM 显示,最大树脂收缩深度取决于树脂宽度和老化时间。树脂收缩曲线的演变证明了树脂裂纹对收缩的加速效应。微观-CIM 显示,宏观纱线裂纹是通过树脂富集区的微观树脂裂纹累积和纤维/树脂界面脱粘形成的。纤维/树脂界面裂纹的形成与树脂收缩状态有关,只有当周围树脂收缩斜率超过特定临界值时才会出现。来源:复合材料力学仿真Composites FEM

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